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العنوان
Preparation, characterization and physical properties of novel nano calcium phosphate to be used in many applications /
الناشر
Mohamed khalaf Ahmed Ammar ,
المؤلف
Mohamed Khalaf Ahmed Ammar
هيئة الاعداد
باحث / Mohamed Khalaf Ahmed Ammar
مشرف / Mohamed Ali Ahmed
مشرف / Salwa Fahim Mansour
مشرف / Soha Mohamed Abdelwahab
تاريخ النشر
2014
عدد الصفحات
182 P. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
الفيزياء والفلك (المتنوعة)
تاريخ الإجازة
30/3/2015
مكان الإجازة
جامعة القاهرة - كلية العلوم - Physics
الفهرس
Only 14 pages are availabe for public view

from 208

from 208

Abstract

In this work, three series of samples were prepared by using the co precipitation and the microwave assisted methods techniques. The first group, calcium phosphate with different Ca/P ratio and different pH values were synthesized. from the X-ray diffraction patterns (XRD) for the samples, it’s clear that the formed phase was brushite at pH 5 and 6 and hydroxyapatite at pH 7, 9 and 12. In the second group, calcium phosphate with Ca/P=1.67 and different pH values (5, 6, 7, 9 and 11) were synthesized. It is clear from XRD that the formed phase was brushite at pH 5 and hydroxyapatite at the other pH values. The high resolution transmission electron microscope (HRTEM) proved that the aspect ratio decreased with the pH values. All the second group were annealed at 800, 1000, 1100 and 1200{u00B0}C. XRD shows wide range of calcium phosphate phases depending on the pH value and the temperature. The microhardness test proved that the mechanical properties enhanced with the pH increasing